lindberg_blue_tube_oven
This is an old revision of the document!
Table of Contents
Oxygen tube oven annealing
The tube oven has a temperature range of up to xxxx °C and can fit 1 inch diameter tubes. Temperature regulation is done by a Lindberg/Blue UP150 controller.
Notes before usage
- read safety notes below
- Keep the components clean and do not use tubes that are not assigned to you
- Make sure to mark or label your tube if you wish to keep it clean and keep it in the cupboard
- Indicate whether samples are loaded or not
- Check the specifications of the tube and boat before usage, make sure your tube and boat are suitable for your process (operating temperature)
- Place all parts in the small boxes near the oven
Tube specifications
Outer diameter: 25mm or 1 inch (25.4mm)
Length: between xxcm and xxcm
Operating temperatures:
- Pyrex: 500°C (greenish color when viewing the edges)
- Quartz: 1000°C
- Al2O3: 1700°C
Safety
Most important safety points are:
- high temperature
- pressurized gas cylinders
High temperature safety
Always lock the oven when a process is running. Let process cool down to 50°C before handling any components. No organic solvents on the table when a process is running. Work with clean tubes
Pressurized gas cylinders safety
Do not attempt to change cylinders or connected equipment, always consult with a technician.
Setting up and starting the process
- check that your tube and sample boat have a higher operating temperature specified than your process temperature
Cool down and finish
- if you operated in single setpoint mode: turn off oven manually
- wait until oven temp is below 50°C before taking out the sample
- close cylinder, keep flow until pressure on primary and secundary pressure gauges are 0.
- close reducer and needle valve
- take out sample and put aluminium foil on parts to keep them clean
Using the UP150 temperature controller
You can operate the temperature controller in two modes:
- single setpoint mode: the controller will go to the desired temperature and maintain the temperature indefinitely, you have to turn the oven off manually
- programming mode: the user can enter a series of setpoint and time values, the controller will follow the sequence.
lindberg_blue_tube_oven.1669280977.txt.gz · Last modified: 2022/11/24 09:09 by scholma