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lindberg_blue_tube_oven

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Oxygen tube oven annealing

The tube oven has a temperature range of up to xxxx °C and can fit 1 inch diameter tubes. Temperature regulation is done by a Lindberg/Blue UP150 controller.

Notes before usage

  • read safety notes below
  • Keep the components clean and do not use tubes that are not assigned to you
  • Make sure to mark or label your tube if you wish to keep it clean and keep it in the cupboard
  • Indicate whether samples are loaded or not
  • Check the specifications of the tube and boat before usage, make sure your tube and boat are suitable for your process (operating temperature)
  • Place all parts in the small boxes near the oven

Tube specifications

Outer diameter: 25mm or 1 inch (25.4mm)
Length: between xxcm and xxcm

Operating temperatures:

  • Pyrex: 500°C (greenish color when viewing the edges)
  • Quartz: 1000°C
  • Al2O3: 1700°C

Safety

Most important safety points are:

  • high temperature
  • pressurized gas cylinders

High temperature safety

Always lock the oven when a process is running. Let process cool down to 50°C before handling any components. No organic solvents on the table when a process is running. Work with clean tubes

Pressurized gas cylinders safety

Do not attempt to change cylinders or connected equipment, always consult with a technician.

Setting up and starting the process

  • check that your tube and sample boat have a higher operating temperature specified than your process temperature

Cool down and finish

  • if you operated in single setpoint mode: turn off oven manually
  • wait until oven temp is below 50°C before taking out the sample
  • close cylinder, keep flow until pressure on primary and secundary pressure gauges are 0.
  • close reducer and needle valve
  • take out sample and put aluminium foil on parts to keep them clean

Using the UP150 temperature controller

You can operate the temperature controller in two modes:

  • single setpoint mode: the controller will go to the desired temperature and maintain the temperature indefinitely, you have to turn the oven off manually
  • programming mode: the user can enter a series of setpoint and time values, the controller will follow the sequence.

Manual UP150 controller

lindberg_blue_tube_oven.1669280977.txt.gz · Last modified: 2022/11/24 09:09 by scholma

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